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The effects of Air/Fuel (A/F) ratios and Exhaust Gas Re-Circulation (EGR) rates on Homogeneous Charge Compression Ignition (HCCI) combustion of n-heptane have been experimentally investigated. The experiments were carried out in a single-cylinder, 4-stroke and variable compression-ratio engine equipped with a port fuel injector. Investigations concentrate on the HCCI combustion of n-heptane at different A/F ratios, EGR rates and their effects on knock limit, engine load, combustion variability, and engine-out emissions such as NOx, CO, and unburned HC. Variations of auto-ignition timings and combustion durations in the two-stage combustion process are analyzed in detail. Results show that HCCI combustion with a diesel type fuel can be implemented at room temperature with a conventional diesel engine compression-ratio. However, its knock limit occurs at very high A/F ratios, although high EGR rates can be tolerated.