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Soot particles emitted from modern diesel engines, despite significantly lower total mass, show higher reactivity and toxicity than black-smoking old engines, which cause serious health and environmental issues. Soot nanostructure, i.e. the internal structure of soot particles composed of nanoscale carbon fringes, can provide useful information to the investigation of the particle reactivity and its oxidation status. This study presents the nanostructure details of soot particles sampled directly from diesel flames in a working diesel engine as well as from exhaust gases to compare the internal structure of soot particles in the high formation stage and after in-cylinder oxidation. Thermophoretic soot sampling was conducted using an in-house-designed probe with a lacy transmission electron microscope (TEM) grid stored at the tip.

The present study focuses on the observation of knock phenomena in a small-bore optical diesel engine. Current understanding is that a drastic increase of pressure during the premixed burn phase of the diesel combustion causes gas cavity resonances, which in turn induce a high frequency pressure ringing. The frequency and severity of this ringing can be easily measured by using a pressure transducer. However, visual information of flames under knocking conditions is limited especially for a small-bore diesel engine. To fill this gap, high-speed imaging of soot luminosity is performed in conjunction with in-cylinder pressure measurement during knocking cycles in an automotive-size optical diesel engine. From the experiments, flames were observed to oscillate against the direction of the swirl flow when the pressure ringing occurred.

In-flame soot sampling based on the thermophoresis of particles and subsequent transmission electron microscope (TEM) imaging has been conducted in a diesel engine to study size, shape and structure of soot particles within the reacting diesel jet. A direct TEM sampling is pursued, as opposed to exhaust sampling, to gain fundamental insight about the structure of soot during key formation and oxidation stages. The size and shape of soot particles aggregate structure with stretched chains of spherical-like primary particles is currently an unknown for engine soot modelling approaches. However, the in-flame sampling of soot particles in the engine poses significant challenges in order to extract meaningful data. In this paper, the engine modification to address the challenges of high-pressure sealing and avoiding interference with moving valves and piston are discussed in detail.

Some soot particles emitted from common-rail diesel engines are so small that can penetrate deep into the human pulmonary system, causing serious health issues. The analysis of nano-scale internal structure of these soot particles sampled from the engine tailpipe has provided useful information about their reactivity and toxicity. However, the variations of carbon fringe structures during complex soot formation/oxidation processes occurring inside the engine cylinder are not fully understood. To fill this gap, this paper presents experimental methods for direct sampling and nanostructure analysis of in-flame soot particles in a working diesel engine. The soot particles are collected onto a lacey carbon-coated grid and then imaged in a high-resolution transmission electron microscope (HR-TEM). The HR-TEM images are post-processed using a Matlab-based code to obtain key nanostructure parameters such as carbon fringe length, fringe-to-fringe separation distance, and fringe tortuosity.

Wall-deposition of soot particles occurs during the cylinder liner wall/flame interaction, which can potentially deteriorate engine oil quality and alter the heat loss rate in a diesel engine. These issues motivate a detailed study on structure and size of the wall-deposited soot particles. A morphological difference between the wall-deposited soot and in-flame soot particles is another focus of this study. We performed thermophoretic soot sampling in the cylinder liner wall using an in-liner-type sampler. Obtained soot particles were imaged by a transmission electron microscope and post-processed to acquire the number of particles, projection area on the sampling grid, and size distribution. The same set of data was also obtained for soot particles within the diesel flame using a probe-type sampler.