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The Major Constituent Analyzer (MCA) is a mass spectrometer-based atmospheric monitoring instrument in the Laboratory Module of the International Space Station (ISS). The MCA is used for continuous environmental monitoring of 6 major gas constituents in the ISS atmosphere as well as safety-critical monitoring for special Environmental Control and Life Support (ECLS) operations such as Pre-Breathe in the Airlock for Extra-Vehicular Activities (EVAs) and oxygen re-pressurizations. For the latter, it is desirable to make most efficient use of consumables by transferring the maximum amount from O2 re-supply tanks on board the shuttle or Progress. The upper safety limit for O2 transfer is constrained by the MCA measurement error bands. A study was undertaken to tighten these error bands and afford NASA-Mission Operations Directorate (MOD) more operational flexibility.