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In support of the National Aeronautics and Space Administration(NASA), a laboratory has been established at the Jet Propulsion Laboratory (JPL) to evaluate the characteristics of chemical sensors which are candidates for use in a controlled chemical processing life support system. Such a facility is required for characterizing those sensors under development as well as those commercially available but whose functional properties are typically based upon operating in industrial environments that will not be completely synonomous with space operations. Space environments, such as an orbiting station or lunar base, will generally have different sensor requirements than terrestrial applications with respect to size, multifunctionality, sensitivity, reliability, temperature, ruggedness, mass, consumables, life, and power requirements. Both commercially available and developmental moisture sensors have been evaluated.

The Mars Exploration Rover (MER) flight system uses mechanical, paraffin-actuated heat switches as part of its secondary battery thermal control system. This paper describes the design, flight qualification, and performance of the heat switch. Although based on previous designs by Starsys Research Corporation1,2, the MER mission requirements have necessitated new design features and an extensive qualification program. The design utilizes the work created by the expansion of a paraffin wax by bringing into contact two aluminum surfaces, thereby forming a heat conduction path. As the paraffin freezes and contracts, compression springs separate the surfaces to remove the conduction path. The flight qualification program involved extensive thermal performance, structural, and life testing.

Passively activated thermal control valves were developed for use in a mechanically pumped single-phase fluid liquid loop (MPFL) of the Mars Science Laboratory (MSL) rover. A key approach to the thermal control of the rover with the fluid loop is to control the flow through the rover's heat generating or heat rejecting components. This is achieved by either splitting or mixing the fluid stream coming from different branches of the system at different temperatures; actively or passively controlled flow valves are typically used for such purposes. To meet the thermal control requirements of the Mars Science Laboratory (MSL) rover, a splitting and a mixing thermal control valves with gradual control capabilities using a linear thermal actuator and a spool was developed at Jet Propulsion Laboratory (JPL). The key feature of these control valves is the balancing of the flow through the various branches of the fluid loop in order to balance the heat loads of the whole thermal system.

The Orbiting Carbon Observatory (OCO) will carry a single science instrument scheduled for launch on an Orbital Sciences Corporation LeoStar-2 architecture spacecraft bus in December 2008. The science objective of the OCO instrument is to collect spaced-based measurements of atmospheric CO2 with the precision, resolution, and coverage needed to identify CO2 sources and sinks and quantify their seasonal variability. The instrument will permit the collection of spatially resolved, high resolution spectroscopic observations of CO2 and O2 absorption in reflected sunlight over both continents and oceans. These measurements will improve our ability to forecast CO2 induced climate change. The instrument consists of three bore-sighted, high resolution grating spectrometers sharing a common telescope with similar optics and electronics.

The capabilities of the JPL Electronic Nose have been expanded to include characteristics required for a Technology Demonstration schedule on the International Space Station (ISS) in 2008-2009 [1,2]. Concurrently, to accommodate specific needs on ISS, the processes, tools and analyses which influence all aspects of development of the device have also been expanded. The Third Generation ENose developed for this program uses two types of sensor substrates, newly developed inorganic and organic sensor materials, redesigned electronics, onboard near real-time data analysis and power and data interfaces specifically for ISS. This paper will discuss the Third Generation ENose with a focus on detection of mercury in the parts-per-billion range.

An array-based sensing system based on 32 polymer/carbon composite conductometric sensors is under development at JPL. Until the present phase of development, the analyte set has focused on organic compounds (common solvents) and a few selected inorganic compounds, notably ammonia and hydrazine. The present phase of JPL ENose development has added two inorganics to the analyte set: mercury and sulfur dioxide. Through models of sensor-analyte response developed under this program coupled with a literature survey, approaches to including these analytes in the ENose target set have been determined.

An array-based sensing system based on polymer-carbon composite conductometric sensors is under development at JPL for use as an environmental monitor in the International Space Station. Sulfur dioxide has been added to the analyte set for this phase of development. Using molecular modeling techniques, the interaction energy between SO2 and polymer functional groups has been calculated, and polymers selected as potential SO2 sensors. Experiment has validated the model and two selected polymers have been shown to be promising materials for SO2 detection.

A technology demonstration propylene Loop Heat Pipe (LHP) has been tested extensively in support of the implementation of this two-phase thermal control technology on NASA’s Earth Observing System (EOS) Tropospheric Emission Spectrometer (TES) instrument. This cryogenic instrument is being developed at the Jet Propulsion Laboratory (JPL) for NASA. This paper reports on the transient characterization testing results showing low frequency temperature oscillations. Steady state performance and model correlation results can be found elsewhere. Results for transient startup and shutdown are also reported elsewhere. In space applications, when LHPs are used for thermal control, the power dissipation components are typically of large mass and may operate over a wide range of power dissipations; there is a concern that the LHP evaporator may see temperature oscillations at low powers and over some temperature range.

A method for determining margins in conceptual-level design via probabilistic methods is described. The goal of this research is to develop a rigorous foundation for determining design margins in complex multidisciplinary systems. As an example application, the investigated method is applied to conceptual-level design of the Mars Exploration Rover (MER) cruise stage thermal control system. The method begins with identifying a set of tradable system-level parameters. Models that determine each of these tradable parameters are then created. The variables of the design are classified and assigned appropriate probability density functions. To characterize the resulting system, a Monte Carlo simulation is used. Probabilistic methods can then be used to represent uncertainties in the relevant models. Lastly, results of this simulation are combined with the risk tolerance of thermal engineers to guide in the determination of margin levels.

The Mars Science Laboratory (MSL1) mission to land a large rover on Mars is being planned for Launch in 2009. As currently conceived, the rover would use a Multi-mission Radioisotope Thermoelectric Generator (MMRTG) to generate about 110 W of electrical power for use in the rover and the science payload. Usage of an MMRTG allows for a large amount of nearly constant electrical power to be generated day and night for all seasons (year around) and latitudes. This offers a large advantage over solar arrays. The MMRTG by its nature dissipates about 2000 W of waste heat. The basic architecture of the thermal system utilizes this waste heat on the surface of Mars to maintain the rover's temperatures within their limits under all conditions. In addition, during cruise, this waste heat needs to be dissipated safely to protect sensitive components in the spacecraft and the rover.

We have elicited a reliable Raman spectral signature for glucose in rabbit aqueous humor across mammalian physiological ranges in a rabbit model stressed by recent myocardial infarction. The technique employs near infrared Raman laser excitation at 785 nm, multivariate analysis, non-linear artificial neural networks and an offset spectra subtraction strategy. Aqueous humor glucose levels ranged from 37 to 323 mg/dL. Data were obtained in 80 uL samples to anticipate the volume constraints imposed by the human and rabbit anterior chamber of the eye. Total sample collection time was 10 seconds with total power delivered to sample of 30 Mw. Spectra generated from the aqueous humor were compared qualitatively to artificial aqueous samples and an excitation offset technique was devised to counteract broadband background noise partially obscuring the glucose signature.

Future planetary science missions planned for Mars are expected to be more complex and thermally challenging than any of the previous missions. For future rovers, the operational parameters such as landing site latitudes, mission life, distance traversed, and rover thermal energy to be managed will be significantly higher (two to five times) than the previous missions. It is a very challenging problem to provide an effective thermal control for the future rovers using traditional passive thermal control technologies. Recent investigations at the Jet Propulsion Laboratory (JPL) have shown that mechanical pump based fluid loops provide a robust and effective thermal control system needed for these future rovers. Mechanical pump based fluid loop (MPFL) technologies are currently being developed at JPL for use on such rovers. These fluid loops are planned for use during spacecraft cruise from earth to Mars and also on the Martian surface operations.

Simultaneous measurements were made for particle releases and off-gassing products produced by heating electrical wires. The wire samples in these experiments were heated to selected temperatures in a heating chamber and responses to vapor releases were recorded by the JPL Electronic Nose (ENose) and an Industrial Scientific ITX gas-monitor; particles released were detected by a TSI P-Trak particle counter. The temperature range considered for the experiment is room temperature (24−26°C) to 500 °C. The results were analyzed by overlapping responses from the ENose, ITX gas sensors and P-Trak, to understand the events (particle release/off-gassing) and sequence of events as a function of temperature and to determine qualitatively whether ENose may be used to detect pre-combustion event markers.

A miniaturized electronic nose has been constructed at JPL in collaboration with Caltech. This array of conductometric sensors has been trained to detect and quantify the presence of vapors in the air; the compounds detected have been found as contaminants in shuttle air. This device has potential application as a miniature, distributed device for monitoring and controlling the constituents in air.

A flight experiment to test the operation of an Electronic Nose developed and built at JPL and Caltech was done aboard STS-95 in October-November, 1998. This ENose uses conductometric sensors made of insulating polymer-carbon composite films; it has a volume of 1.7 liters, weighs 1.4 kg including the operating computer and operates on 1.5 W average power. In the flight experiment, the ENose was operated continuously for 6 days and recorded the sensors' response to changes in air in the mid-deck of the orbiter. The ENose had been trained to identify and quantify ten common contaminants at the 24-hour Spacecraft Maximum Allowable Concentration (SMAC) level. Most SMACs are on the order of 10-100 ppm. The experiment was controlled by collecting air samples daily and analyzing them using standard analytical techniques after the flight. The device is microgravity insensitive.

This paper describes results acquired from E-Tongue 2 and E-Tongue 3 which are arrays of planar three-element electrochemical cells and pH sensors. The approach uses ASV (Anodic Stripping Voltammery) to achieve a detection limit, which in the case of Pb, is below one μM which is needed for water quality measurements. The richness of the detectable species is illustrated with Fe where seven species are identified using the Pourbiax diagram. The detection of multiple species is illustrated using Pb and Cu. The apparatus was used to detect the electroactivity of the metabolic-surrogate, PMS (phenazine-methosulphate). Finally, four types of pH sensors were fabricated and characterized for linearity, sensitivity, and responsiveness.

As a result of the Viking missions in 1970s, the presence of a strong oxidant in Martian soil was suggested. Here we present a testable, by near-term missions, hypothesis that iron(VI) contributes to that oxidizing pool. Ferrate(VI) salts were studied for their spectral and oxidative properties and biological activities. Ferrate(VI) has distinctive spectroscopic features making it available for detection by remote sensing reflectance spectra and contact measurements via Mössbauer spectroscopy. The relevant miniaturized instrumentation has been developed or is underway, while XANES spectroscopy is shown to be a method of choice for the returned samples. Ferrate(VI) is capable of splitting water to yield oxygen, and oxidizing organic carbon to CO2. Organic oxidation was strongly abated after pre-heating ferrate, similar to the observations with Mars soil samples.

Phoenix, NASA's first Mars Scouts mission, will be launched in 2007 and will soft-land inside the Martian Arctic Circle, between north 65° and 72° North latitude, in 2008 to study the water history and to search for habitable zones. Similar to the IDD (Instrument Deployment Device) on the Mars Exploration Rovers (MER), Phoenix has a Robotic Arm (RA) which is equipped with a scoop to dig into the icy soil and to deliver the soil samples to instruments for scientific observations and measurements. As with MER, the actuators and the bearings of the Phoenix RA in a non-operating condition can survive the cold Martian night without any electrical power or any thermal insulation. The RA actuators have a minimum operating allowable flight temperature (AFT) limit of -55°C, so, warm-up heaters are required to bring the temperatures of all the RA actuators above the operating AFT limit prior to early morning operation.

The Moon Mineralogy Mapper (M3) instrument is one in a suite of twelve instruments which will fly onboard the Indian Chandrayaan-1 spacecraft scheduled for launch in 2008. Chandrayaan-1 is India's first mission to the Moon and is being managed by the Indian Space Research Organization (ISRO) in Bangalore, India. Chandrayaan-1 overall scientific objective is the photo-selenological and the chemical mapping of the Moon. The primary science objective of the M3 instrument is the characterization and mapping of the lunar surface composition in the context of its geologic evolution. Its primary exploration goal is to assess and map the Moon mineral resources at high spatial resolution to support future targeted missions. It is a “push-broom” near infrared (IR) imaging spectrometer with spectral coverage of 0.4 to 3.0 μm at 10 nm resolution with high signal to noise ratio, spatial and spectral uniformity.

This paper describes a novel thermal control system for future Mars landers and rovers designed to keep battery temperatures within the −10 °C to +25 °C temperature range. To keep the battery temperatures above the lower limit, the system uses: 1) a phase change material (PCM) thermal storage module to store and release heat and 2) a loop heat pipe (LHP) to transfer heat from a set of Radioisotope Heater Units (RHUs) to the battery. To keep the battery temperature below the upper limit, a thermal control valve in the LHP opens to redirect the working fluid to an external radiator where excess heat is dumped to the atmosphere. The PCM thermal storage module was designed and fabricated using dodecane paraffin wax (melting point, − 9.6 °C) as the phase change material. A miniature ammonia loop heat pipe with two condensers and an integrated thermal control valve was designed and fabricated for use with the PCM thermal storage unit.