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The present study was carried out to analyze the catalytic action of K2O-Al2O3 in NOx Storage and Reduction (NSR) monolith catalyst and Fe2O3-TiO2 in Selective Catalytic Reduction (SCR) monolith catalyst. The core objective of this investigation is to determine the maximum percentage of Oxides of Nitrogen (NOx) reduction in NSR and NSR-SCR combined system with respect to engine exhaust gas temperature and compares the results with the results of the conventional mode of operation. To accomplish this task monolith ceramic bricks were coated with K2O-Al2O3 (NSR) and Fe2O3-TiO2 (SCR) catalyst and were placed in different configurations inside the catalytic chamber. Several trials were attempted to get the optimal operating temperature that has a maximum NOx removal efficiency when successively connecting a single NSR catalyst and the combined NSR-SCR double bed catalyst. Single NSR monolith at 320 °C, showed the best NOx conversion rate of 74%.