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Technical Paper

Monitoring Pre-Combustion Event Markers by Heating Electrical Wires

2009-07-12
2009-01-2543
Simultaneous measurements were made for particle releases and off-gassing products produced by heating electrical wires. The wire samples in these experiments were heated to selected temperatures in a heating chamber and responses to vapor releases were recorded by the JPL Electronic Nose (ENose) and an Industrial Scientific ITX gas-monitor; particles released were detected by a TSI P-Trak particle counter. The temperature range considered for the experiment is room temperature (24−26°C) to 500 °C. The results were analyzed by overlapping responses from the ENose, ITX gas sensors and P-Trak, to understand the events (particle release/off-gassing) and sequence of events as a function of temperature and to determine qualitatively whether ENose may be used to detect pre-combustion event markers.
Journal Article

Off-Gassing and Particle Release by Heated Polymeric Materials

2008-06-29
2008-01-2090
Polymers are one of the major constituents in electrical components. A study investigating pre-combustion off-gassing and particle release by polymeric materials over a range of temperatures can provide an understanding of thermal degradation prior to failure which may result in a fire hazard. In this work, we report simultaneous measurements of pre-combustion vapor and particle release by heated polymeric materials. The polymer materials considered for the current study are silicone and Kapton. The polymer samples were heated over the range 20 to 400°C. Response to vapor releases were recorded using the JPL Electronic Nose (ENose) and Industrial Scientific's ITX gas monitor configured to detect hydrogen chloride (HCl), carbon monoxide (CO) and hydrogen cyanide (HCN). Particle release was monitored using a TSI P-TRAK particle counter.
Technical Paper

Thermal Vacuum Testing of the Orbiting Carbon Observatory Instrument

2008-06-29
2008-01-2036
The Orbiting Carbon Observatory (OCO) instrument is scheduled for launch onboard an Orbital Sciences Corporation LEOStar-2 architecture spacecraft in December 2008. The instrument will collect data to identify CO2 sources and sinks and quantify their seasonal variability. OCO observations will permit the collection of spatially resolved, high resolution spectroscopic observations of CO2 and O2 absorption in reflected sunlight over both continents and oceans. OCO has three bore-sighted, high resolution, grating spectrometers which share a common telescope with similar optics and electronics. A 0.765 μm channel will be used for O2 observations, while the weak and strong CO2 bands will be observed with 1.61 μm and 2.06 μm channels, respectively. The OCO spacecraft circular polar orbit will be sun-synchronous with an inclination of 98.2 degrees, mean altitude of 705 km and 98.9 minute orbit period.
Journal Article

ATCC 29669 Spores Show Substantial Dry Heat Survivability

2008-06-29
2008-01-1982
Bacillus sp. ATCC 29669 was isolated from microbial fallout in clean rooms during the assembly of the Viking Spacecraft missions to Mars, making it a potential contamination concern for outbound space missions. Spores from this bacterial strain were found to be thirty times more resistant to dry heat than B. atrophaeus. Spore inactivation rates under vacuum controlled humidity were faster than rates obtained under ambient humidity. Inactivation rates for these heat resistant spores are important considerations for planetary protection implementation where temperature, time and humidity conditions are used to estimate the effectiveness of dry heat microbial reduction (DHMR) procedures.
Technical Paper

Results from the Vehicle Cabin Atmosphere Monitor: A Miniature Gas Chromatograph/Mass Spectrometer for Trace Contamination Monitoring on the ISS and Orion

2008-01-29
2008-01-2045
Progress on the delivery of the Vehicle Cabin Atmosphere Monitor (VCAM) is reported. VCAM is an autonomous trace-species detector to be used aboard the International Space Station (ISS) for atmospheric analysis. The instrument is based on a low-mass, low-power miniature preconcentrator, gas chromatograph, and Paul ion trap mass spectrometer (PCGC/MS) capable of measuring volatile constituents in a space vehicle or planetary outpost at sub-ppm levels. VCAM detects and quantifies 40 target compounds at their 180-day Spacecraft Maximum Allowable Concentration (SMAC) levels. It is designed to operate autonomously, maintenance-free, with a self-contained carrier and calibration gas supplies sufficient for a one-year lifetime. Two flight units will be delivered for operation in the ISS EXPRESS rack.
Technical Paper

Overview of the Vehicle Cabin Atmosphere Monitor, a Miniature Gas Chromatograph/Mass Spectrometer for Trace Contamination Monitoring on the ISS and CEV

2007-07-09
2007-01-3150
Work is underway to deliver an instrument for analysis of the atmosphere aboard the International Space Station. The Vehicle Cabin Atmosphere Monitor (VCAM) is based on a low-mass, low-power miniature preconcentrator gas chromatograph/mass spectrometer (PCGC/MS) capable of providing sub-ppm measurements of volatile constituents in a space vehicle or outpost. VCAM is designed to operate autonomously, maintenance-free, once per day, with its own carrier and calibration gas supplies sufficient for a one-year lifetime. VCAM performance is sufficient to detect and identify 90% of the target compounds specified at their 180-day Spacecraft Maximum Allowable Concentration (SMAC) levels. The flight units will be delivered in mid-2008 and be operated in the ISS EXPRESS rack.
Technical Paper

Viral Populations within the International Space Station's Internal Active Thermal Control System Ground Support and Potential Flight Hardware

2007-07-09
2007-01-3108
The Internal Active Thermal Control System (IATCS) aboard the International Space Station (ISS) contains an aqueous, alkaline fluid (pH 9.5±0.5) that aids in maintaining a habitable environment for the crew. Because microbes have significant potential to cause disease, adverse effects on astronaut health, and microbe-induced corrosion, the presence of both bacteria and viruses within IATCS fluids is of concern. This study sought to detect and identify viral populations in IATCS samples obtained from the Kennedy Space Center as a first step towards characterizing and understanding potential risks associated with them. Samples were concentrated and viral nucleic acids (NA) extracted providing solutions containing 8.87-22.67 μg NA per mL of heat transfer fluid. After further amplification viral DNA and cDNA were then pooled, fluorescently labeled, and hybridized onto a Combimatrix panvira 12K microarray containing probes for ∼1,000 known human viruses.
Technical Paper

Mechanically Pumped Fluid Loop Technologies for Thermal Control of Future Mars Rovers

2006-07-17
2006-01-2035
Future planetary science missions planned for Mars are expected to be more complex and thermally challenging than any of the previous missions. For future rovers, the operational parameters such as landing site latitudes, mission life, distance traversed, and rover thermal energy to be managed will be significantly higher (two to five times) than the previous missions. It is a very challenging problem to provide an effective thermal control for the future rovers using traditional passive thermal control technologies. Recent investigations at the Jet Propulsion Laboratory (JPL) have shown that mechanical pump based fluid loops provide a robust and effective thermal control system needed for these future rovers. Mechanical pump based fluid loop (MPFL) technologies are currently being developed at JPL for use on such rovers. These fluid loops are planned for use during spacecraft cruise from earth to Mars and also on the Martian surface operations.
Technical Paper

Expanding the Capabilities of the JPL Electronic Nose for an International Space Station Technology Demonstration

2006-07-17
2006-01-2179
An array-based sensing system based on polymer-carbon composite conductometric sensors is under development at JPL for use as an environmental monitor in the International Space Station. Sulfur dioxide has been added to the analyte set for this phase of development. Using molecular modeling techniques, the interaction energy between SO2 and polymer functional groups has been calculated, and polymers selected as potential SO2 sensors. Experiment has validated the model and two selected polymers have been shown to be promising materials for SO2 detection.
Technical Paper

Self-Deployable Foam Antenna Structures for Earth Observation Radiometer Applications

2006-07-17
2006-01-2064
The overall goal of this program was the development of a 10 m. diameter, self-deployable antenna based on an open-celled rigid polyurethane foam system. Advantages of such a system relative to current inflatable or self-deploying systems include high volumetric efficiency of packing, high restoring force, low (or no) outgassing, low thermal conductivity, high dynamic damping, mechanical isotropy, infinite shelf life, and easy fabrication with methods amenable to construction of large structures (i.e., spraying). As part of a NASA Phase II SBIR, Adherent Technologies and its research partners, Temeku Technologies, and NASA JPL/Caltech, conducted activities in foam formulation, interdisciplinary analysis, and RF testing to assess the viability of using open cell polyurethane foams for self-deploying antenna applications.
Technical Paper

Expanding the Analyte Set of the JPL Electronic Nose to Include Inorganic Species

2005-07-11
2005-01-2880
An array-based sensing system based on 32 polymer/carbon composite conductometric sensors is under development at JPL. Until the present phase of development, the analyte set has focused on organic compounds (common solvents) and a few selected inorganic compounds, notably ammonia and hydrazine. The present phase of JPL ENose development has added two inorganics to the analyte set: mercury and sulfur dioxide. Through models of sensor-analyte response developed under this program coupled with a literature survey, approaches to including these analytes in the ENose target set have been determined.
Technical Paper

Microbial Burden of Commercial Aircraft Cabin Air

2005-07-11
2005-01-3087
The microbial burdens of 69 cabin air samples collected in-flight aboard commercial airliners were assessed via culture-dependent and molecular-based microbial enumeration assays. Cabin air samples from each of four separate flights aboard two different carriers were collected via air-impingement. Microbial enumeration techniques targeting DNA, ATP, and endotoxin were employed to estimate total microbial burden. The total viable microbial population ranged from 0 to 3.6 × 104 cells per 100 liters of air, as assessed by the ATP-assay. When these same samples were plated on minimal medium, anywhere from 2 to 80% of the viable population was cultivable. Five of the 29 samples examined exhibited higher cultivable plate counts than ATP-derived viable counts, perhaps a consequence of the dormant nature (lower concentration of intracellular ATP) of cells inhabiting these air cabin samples.
Technical Paper

Extended Temperature Range Studies for Dry Heat Microbial Reduction

2005-07-11
2005-01-3096
Dry heat microbial reduction is an approved method to reduce the microbial bioburden on space-flight hardware prior to launch to meet flight project planetary protection requirements. Microbial bioburden reduction also occurs if a spacecraft enters a planetary atmosphere (e.g., Mars) and is heated by frictional forces. However, without further studies, administrative credit for this reduction cannot be applied. The killing of Bacillus subtilis var. niger spores has been examined and lethality data has been collected by placing spores in a vacuum oven or thermal spore exposure vessels (TSEV) in a constant temperature bath. Using this lethality data, a preliminary mathematical model is being developed that can be used to predict spore killing at different temperatures. This paper will present the lethality data that has been collected at this time and the planned future studies.
Technical Paper

Q-PCR Based Bioburden Assessment of Drinking Water Throughout Treatment and Delivery to the International Space Station

2005-07-11
2005-01-2932
Previous studies indicated evidence of opportunistic pathogens in samples obtained during missions to the International Space Station (ISS). This study utilized TaqMan quantitative PCR to determine specific gene abundance in potable and non-potable ISS waters. Probe and primer sets specific to the small subunit rRNA genes were designed and used to elucidate overall bacterial rRNA gene numbers. In addition, primer-probe sets specific for Burkholderia cepacia and Stenotrophomonas maltophilia were optimized and genes of these two opportunistic pathogens quantified in the pre- and post-flight drinking water as well as coolant waters. This Q-PCR approach supports findings of previous culture-based studies however; the culture based studies may have underestimated the microbial burden of ISS drinking water.
Technical Paper

Implications of the VBNC State of B. cepacia and S. maltophilia on Bioreduction and Microbial Monitoring of ISS Potable Waters

2005-07-11
2005-01-2933
Certain Eubacteria enter a viable but nonculturable (VBNC) state upon encountering unfavorable environmental conditions. VBNC cells do not divide on conventional media yet remain viable and in some cases retain virulence. Here, we describe the VBNC state of two opportunistic pathogens previously isolated from ISS potable waters, Burkholderia cepacia and Stenotrophomonas maltophilia. Artificially inoculated microcosms were exposed to the biocidal agents copper (CuSO4) and iodine (I2) in an attempt to induce nonculturablility. Viability was assessed via fluorescent microscopy (direct viable count assay coupled with BacLight™ staining) and metabolic activity was monitored by quantifying both intracellular ATP and transcribed rRNA (reverse transcriptase quantitative PCR). Culturablility was lost in both B. cepacia and S. maltophilia within two days of exposure to copper or high concentrations of iodine (6 or 8 ppm).
Technical Paper

Mid-IR Semiconductor Lasers for Chemical Sensing

2003-07-07
2003-01-2551
The development of mid-IR semiconductor diode lasers based on type-II interband cascade structures is presented. How these diode lasers can be developed to meet the requirements in chemical sensing applications is discussed.
Technical Paper

Thermal Performance Evaluation of a Small Loop Heat Pipe for Space Applications

2003-07-07
2003-01-2688
A Small Loop Heat Pipe (SLHP) featuring a wick of only 1.27 cm (0.5 inches) in diameter has been designed for use in spacecraft thermal control. It has several features to accommodate a wide range of environmental conditions in both operating and non-operating states. These include flexible transport lines to facilitate hardware integration, a radiator capable of sustaining over 100 freeze-thaw cycles using ammonia as a working fluid and a structural integrity to sustain acceleration loads up to 30 g. The small LHP has a maximum heat transport capacity of 120 Watts with thermal conductance ranging from 17 to 21 W/°C. The design incorporates heaters on the compensation chamber to modulate the heat transport from full-on to full-stop conditions. A set of start up heaters are attached to the evaporator body using a specially designed fin to assist the LHP in starting up when it is connected to a large thermal mass.
Technical Paper

Evaluation of Sample Preservation Methods for Space Missions

2003-07-07
2003-01-2671
This study of samples collected from Mars 01 Orbiter was conducted to gain a better understanding and practical experience in methods to process and preserve samples intended for planetary protection analysis. Samples were evaluated for the viable growth of microbes, the molecular biomarker adenosine triphosphate (ATP), and the presence of lipopolysaccharide, a bacterial cell wall component. Losses were observed in the number of viable microbes after freezing as well as in the detectable lipopolysaccharide. Two independent studies of pooled cleanroom samples demonstrate good ATP recovery and consistent values after freezing at −20 °C.
Technical Paper

Design and Flight Qualification of a Paraffin-Actuated Heat Switch for Mars Surface Applications

2002-07-15
2002-01-2275
The Mars Exploration Rover (MER) flight system uses mechanical, paraffin-actuated heat switches as part of its secondary battery thermal control system. This paper describes the design, flight qualification, and performance of the heat switch. Although based on previous designs by Starsys Research Corporation1,2, the MER mission requirements have necessitated new design features and an extensive qualification program. The design utilizes the work created by the expansion of a paraffin wax by bringing into contact two aluminum surfaces, thereby forming a heat conduction path. As the paraffin freezes and contracts, compression springs separate the surfaces to remove the conduction path. The flight qualification program involved extensive thermal performance, structural, and life testing.
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